iso 9001:2000 registered certificate 77689 1/5/2001 technical support please call our technical support group for any questions where an experienced staff member will assist you with your order 1-800-220-5171 ext.626 or email spectroscopy@wilmad-labglass.com international callers dial 856-697-3000 ext.626 email international@spindustries.com or contact your local authorized wilmad/labglass distributor explan at ionofconcentricityandcambermeasurementsanditsimpo rta nceforthenmrspectroscopist concentricity is defined as a measure of the lack of uniformity of the wall-thickness of the tube this tolerance can be thought of as the degree to which the cylinders as defined by the inner and outer surfaces of the tube parallel and overlap determined using an indicating gauge this tolerance is reported as a deviation ± or total indicator reading t.i.r i.e the absolute variation in wall thickness at the ends of a tube being rotated through 360 degrees ideally zero tubes which conform to t.i.r
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10mm od nmr tubes thin walled pyrex® or equivalent glass mhz product no rating 513-7pp-7 513-7pp-8 513-7pp-9 513-5pp-7 513-5pp-8 513-5pp-9 513-3pp-7 513-3pp-8 513-3pp-9 513-1pp-7 513-1pp-8 513-1pp-9 513-1ps-7 513-1ps-8 513-1ps-9 500 500 500 400 400 400 300 300 300 200 200 200 100 100 100 length wall concentricity inch thickness mm microns 7 8 9 7 8 9 7 8 9 7 8 9 7 8 9 0.46 0.46 0.46 0.46 0.46 0.46 0.46 0.46 0.46 0.46 0.46 0.46 0.46 0.46 0.46 38 38 38 51 51 51 76 76 76 254 254 254 nominal nominal nominal camber microns 13 13 13 25 25 25 38 38 38 51 51 51 nominal nominal nominal concentricity camber tolerance inch t.i.r inch t.i.r od/id 0.0015 0.0015 0.0015 0.002 0.002 0.002 0.003 0.003 0.003 0.01 0.01 0.01 nominal nominal nominal 0.0005 0.0005 0.0005 0.001 0.001 0.001 0.0015 0.0015 0.0015 0.002 0.002 0.002 nominal nominal nominal c/d c/d c/d c/d c/d c/d c/d c/d c/d c/d c/d c/d e/e e/e e/e 10mm od nmr tubes ultra thin walled pyrex® or equivalent glass mhz product no rating 513-7ppx
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pyrex® nmr capillary short capillary tubes 10 pieces per pack product no wg-1364-1 wg-1364-1.7 wg-1364-1.9 wg-1364-2 wg-1364-2.5a these capillaries are sealed at one end standard capillary tubes 5 pieces per pack product no wg-1364-1-203m wg-1364-1.7-203m wg-1364-2-203m wg-1364-2.5a-203m these capillaries are sealed at one end long capillary tubes packaging per customer option product no wg-1365-1 wg-1365-1.7 wg-1365-1.9 wg-1365-2 wg-1365-2.5a both ends open od mm 1 1.7 1.9 2 2.5 id mm .8 1.3 1.5 1.6 2.2 length mm 300 300 300 300 300 od mm 1 1.7 1.9 2 2.5 id mm .8 1.3 1.5 1.6 2.2 length mm 75 100 110 100 100 use capillary tubes and inserts for your smallest samples od mm 1 1.7 2 2.5 id mm .8 1.3 1.6 2.2 length mm 203 203 203 203 you can use our wg-1364 capillary tubes for the simplest external reference experiments just seal the reference in the capillary and drop it into your sample tube great for non-spinning experiments or use wilmad s wg-1365 capillaries as inserts with our ptfe
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22 www.wilmad-labglass.com 22
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doty susceptibility plugs for nmr microsampling · easier to use than the glass alternative · can be used with a wider range of solvents · use them with existing tubes · lower in cost than glass · less fragile than susceptibility-altered glass microtubes traditionally sample sizes were 3-5 times the height of the probe r coil all magnetic field distortions caused by magnetic susceptibility discontinuities at the upper air-sample and lower glass-sample interfaces were far from the sensitive probe r coil region small samples diluted to larger traditional volumes 1 ml yield poor nmr spectra in high field spectrometers through magnetic susceptibility matching of the sample solvent doty susceptibility plugs allow the sample to be substantially concentrated by extending out the air-sample/glass sample interfaces far enough away from the r coil region to remove the magnetic field distortions doty susceptibility plugs are provided as sets of two positioning rod and collar are provided as a set
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doty product no wp-501-5135 wp-601-5135 wp-501-5150 wp-601-5150 wp-501-7185 wp-601-7185 wp-501-7222 wp-601-7222 sold/each description zro2 mas rotor 5mm od x 13mm long kel-f cap short for 5mm od ambient temperature zro2 mas rotor 5mm od x 15mm long kel-f cap short for 5mm od ambient temperature zro2 mas rotor 7mm od x 18.5mm long kel-f cap short for 7mm od ambient temperature zro2 mas rotor 7mm od x 22.2mm long kel-f cap short for 7mm od ambient temperature probe 5mm standard 5mm standard 5mm high speed 5mm high speed 7mm standard 7mm standard 7mm high speed 7mm high speed pyrex® mas rotor inserts for air-sensitive samples and semi-solid samples such as gels or highly viscous liquids the sample is simply sealed into the insert tube by heat-sealing with a torch or by applying a small drop of epoxy to the constriction after the epoxy is set and dry the sealed insert is then cut through the constriction with a glass saw using a small funnel powder samples can be packed into the insert
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46 tube size parameter set-up sensitivity sensitivity sensitivity sensitivity sensitivity sensitivity sensitivity wgh-42-2.5 wgh-46-2.5 wgh-54-2.5 wgh-11-2.5 wgh-28-2.5 wgh-111-2.5 wgh-106-2.5 wgh-42-3 wgh-46-3 wgh-54-3 wgh-11-3 wgh-28-3 wgh-111-3 wgh-106-3 wgh-42-3-8 wgh-46-3-8 wgh-54-3-8 wgh-11-3-8 wgh-28-3-8 wgh-111-3-8 wgh-106-3-8 wgh-42-5 wgh-46-5 wgh-54-5 wgh-11-5 wgh-28-5 wgh-111-5 wgh-106-5 wgh-42-5-8 wgh-46-5-8 wgh-54-5-8 wgh-11-5-8 wgh-28-5-8 wgh-111-5-8 wgh-106-5-8 wgh-42-8 wgh-46-8 wgh-54-8 wgh-11-8 wgh-28-8 wgh-111-8 wgh-106-8 wgh-42-8-8 wgh-46-8-8 wgh-54-8-8 wgh-11-8-8 wgh-28-8-8 wgh-111-8-8 wgh-106-8-8 wgh-42-10 wgh-46-10 wgh-54-10 wgh-11-10 wgh-28-10 wgh-111-10 wgh-106-10 wgh-42-10-8 wgh-46-10-8 wgh-54-10-8 wgh-11-10-8 wgh-28-10-8 wgh-111-10-8 wgh-106-10-8 proton 1h 2.5mm 8 3mm 7 3mm 8 5mm 7 5mm 8 8mm 7 8mm 8 10mm 7 10mm 8 5mm coaxial product no description proton 1h 10mm coaxial wgh-42 wgh-46 wgh-54 wgh-11 wgh-28 wgh-111 wgh-106 wgh-42-5c wgh-42-10c wgh-46-
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54 formula 1.12 0.87 d-13-100g cd3cood cd3cocd3 17 -94 118 57 d-11-10g d-13-10g d-121-10g d-152-10g d-129-5g 0.84 0.95 d-21-100g d-130 5ml d-28-50g d-28-100g d-31-50g d-31-100g d-153-50g d-153-100g d-131-50g d-36-50g d-110-50g d-39-100g d-87-100g d-136-100g d-133-10g d-134-10g d-141-10g d-133-50g d-133 5ml d-39 75ml d-130-5g 1.50 -64 62 -45 5 82 80 d-14-10g d-21-10g d-122-10g d-14-25g d-21-25g d-122-25g d-14-50g d-21-50g d-122-50g d-129 5ml d-13 75ml d-121 75ml d-152 75ml d-129 75ml d-14 75ml d-21 75ml d-11-25g d-13-25g d-121-25g d-152-25g d-11-50g d-13-50g d-121-50g d-152-50g deuterated solvents min.iso density purity d g/ml 1g 5g 10g 25g 50g 100g 10x0.5ml 10x0.75ml mp °c bp °c 5xlg product no description cd3cn c6d6 cdcl3 d-131 5ml d-130 75ml d-28 75ml d-31 75ml d-153 75ml d-131 75ml d-137-lg c6d12 dcl d2o 3.8 www.wilmad-labglass.com 0.89 1.25 1.20 1.11 6 81 108 108 101.4 d-137-1g d-137-5g d-131-10g d-137-10g 99.996 d-141-50g d-141 5ml 99.5 1.18 18 189 1.04 -61 153 d-84-lg d-84-5g d-8
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combination ph electrode for use in 5mm thin wall nmr sample tubes up to 8 in length glass probe dimensions are 3mm od x 180mnm long ph range 0-14 temperature range 0-70°c resolution 0.02 ph units sodium error 0.1 at ph 12 resistance at 20°c 100-1000 megohims reproducibility 99 within note wilmad sleeve adapter set product no wg-1132-4 can be used to adapt the electrode to a 10mm od sample tube connectors 6030-02-bnc 6030-02-3 6030-02-6 product no 6030-02-bnc 6030-02-3 6030-02-6 description ph electrode with bnc connector ph electrode with #3 american std connector ph electrode with 6mm radiometer connector electrode solutions packaged in 125ml bottles product no 18513 18823 18528 18508 18895 description reference solution-3m kci saturated with agci electrode storage solution-3m kci diaphragm cleaner-thiol based electrode cleaner-for removing protein coating reactivating solution-hydrofluoric acid based special connector adapters if you have a bnc electrode these special adapters
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ultrasonic cleaning systems product no sc-101 sc-101t sc-101h sc-101th sc-101-22 sc-101t-22 sc-101h-22 sc-101th-22 description ultrasonic cleaner ultrasonic cleaner with 0-30 minute timer ultrasonic cleaner with heater ultrasonic cleaner with 0-30 minute timer and heater ultrasonic cleaner 220v ultrasonic cleaner with 0-30 minute timer 220v ultrasonic cleaner with heater 220v ultrasonic cleaner with 0-30 minute timer and heater 220v accessories product no c-100 b-101 it-101 wg-11100 description stainless steel cover stainless steel basket stainless steel tray-liquid tight nmr tube rack-poly coated detergents product no 101 ic-11 description alkaline cleaning concentrate 1 part to 30 parts water detergent cleaner concentrate it-101 our ultrasonic cleaners have a 1 gallon capacity tube cleaning rack is plastic-coated to protect tubes b101 wg-11100 the ultrasonic cleaning systems are used for cleaning stubborn chemical stains inside nmr tubes where test tube brushes should not be
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935 mearns road warminster pa 18974 · usa tel 800-523-2327 tel 215-672-7800 fax 215-672-7807 www.spindustries.com sp techcare rt 40 oak road buena nj 08310 · usa tel 800-220-5171 tel 856-697-3000 fax 856-697-0536 www.wilmad-labglass.com 935 mearns road warminster pa 18974 · usa tel 877-548-4666 tel 215-672-7800 fax 215-672-1702 www.sptechcare.com 935 mearns road warminster pa 18974 · usa tel 800-523-3608 tel 215-672-7800 fax 215-672-7807 www.hotpack.com 815 route 208 gardiner ny 12525-9989 · usa tel 800-431-8232 tel 845-255-5000 fax 845-255-5338 www.virtis.com 935 mearns road warminster pa 18974 · usa tel 800-523-2327 tel 215-672-7800 fax 215-672-7807 www.hullcompany.com sales email cs@wilmad-labglass.com · tech support email spectroscopy@wilmad-labglass.com
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